Based on dissolution of a test sample in water. Distillation of the ammonia after displacement by an alkali solution. Absorption in an excess of standard volumetric sulphuric acid solution and back-titration with standard volumetric sodium hydroxide solution in the presence of methyl red/methylene blue mixed indicator. A typical distillation apparatus is shown in a figure.
Status : WithdrawnPublication date : 1975-07
Edition : 1Number of pages : 4