This standard has been reviewed* and then confirmed in 2009.
Specifies the determination for natural and synthetic materials having a molar ratio sodium fluoride/aluminium trifluoride between 3 and 1,7 approximately. The principle consists in fusion of a test portion with sodium carbonate, separation of fluorine by distillation with sulphuric acid or perchloric acid. Titration with thorium nitrate solution in presence of sodium alizarinsulphonate/methylene blue as indicator. Alternatively, the thorium nitrate titration may be made using only sodium alizarinsulphonate, the end-point being*spectrophotometrically determined at 525 nm.
Edition: 1 (Monolingual) ICS: 71.060.50 Status: Published Stage: 90.20 (2014-07-15) TC/SC: ISO/TC 226 Number of Pages: 6
No revision information available
No corrigenda or amendments available